Introduction: Thyme contains a surprising amount of iron compounds. This essay enables us to determine the amount of iron(II) present in modify thyme by means of a redox reaction. Method: 1. iron accurately ab proscribed 1g of dried thyme and put into a 250cm3 beaker. enroll the mass of thyme used. 2. employ a measuring cylinder, add 50cm3 of 1.0mol dm-3 sulphuric(VI) acerbic and boil gently for 5 minutes. 3. Allow the mixture to unbosom for a few minutes then filter it, victimization either gravity or vacuum filtration. (We shall be victimisation vacuum filtration.) Wash the residue in the funnel at a time with a little water and store all the filtrate. 4. displace all the filtrate and washings into a 250cm3 volumetrical flaskful. Make up to 250cm3 with 1.0mol dm-3 sulphuric hot(VI) acid. Stopper the flask and repeal several measure to thoroughly mix the solution. 5. Fill the buret with 0.005mol dm-3 potassium mangana te(VII) solution. 6. displace some of the thyme extract solution into a 250cm3 plastic beaker. 7. using a measuring cylinder, add 50cm3 of 1.0mol dm-3 sulphuric(VI) acid to the thyme extract in the conical flask. 8. Titrate the solution in the conical flask with the potassium manganate(VII) solution until a lookout pink colouration persists for 10 seconds. 9. Repeat the titration until there ar two titres at heart 0.1cm3 of each other.
Record results in a suitable table. Results: close to askher(p) Titre: 7.653 First travel by: 6.553 Second Run: 6.453 trio Run : 6.553 Calculations: During the titr! ation, iron(II) ions are oxidized to iron(III) ions and manganate(VII) ions are reduced to manganese(II) ions. The comparability is as follows: 5Fe2+(aq) + MnO4-(aq) + 8H+(aq) ? 5Fe3+(aq) + Mn2+(aq) + 4H2O(l) The above equation shows that one mole of manganate(VII) ions reacts with 5 moles of iron(II) ions in acid solution. Using our average titre of 6.52cm3 we mustiness first work out how many moles of potassium manganate(VII) are used. Moles in a...If you want to get a full essay, sound out it on our website: OrderCustomPaper.com
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